TEM

Lab Locations

1121-1151 Engineering Hall

Lab Contacts

Dr. Toshihiro Aoki

Dr. Li Xing

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9-1-1

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(949) 824-5223

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(714) 456-6123

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JEM-ARM300F Grand ARM TEM

Description

The JEOL Grand ARM is 60-300 kV S/TEM, which offers sub-Ångstrom spatial resolution at 300 kV for atom-by-atom characterization and chemical mapping. Equipped with a cold field emission gun and configured with a wide gap pole piece (>6 mm), the Grand ARM is an ideal instrument for a variety of in situ experiments to study the structure, properties, and dynamic behavior of nanostructured materials under applied fields, stress, and reactive environments.

The Grand ARM uses a unique hybrid high-angle annular dark-field (HAADF) STEM detector and features a dedicated annular bright-field (ABF) detector. This capability is critical for the atomic-scale structure and property analysis of materials containing both light and heavy elements. In addition, the Grand ARM is integrated with a new generation direct electron detection system (the Gatan K2 IS/Summit), which enables rapid imaging (up to 1600fps), 4D-STEM, low-dose imaging, and counting EELS.

Also, the microscope is equipped with a Gatan OneView camera (4K x 4K) for optimum imaging, biprism for electron holography, dual 100 mm2 silicon drift detectors (SDD) for energy-dispersive X-ray spectroscopy (EDS), and Gatan 965 GIF Quantum ER imaging filter with dual-energy range EELS (DualEELS), suitable for the rapid mapping of elements with atomic resolution.

Instrument Features

  • Atomic resolution S/TEM imaging and spectroscopy at 60, 80, 200, and 300kV using HAADF, MAADF, BF or ABF, BEI detectors
  • Dual 100mm2 SDDs for super rapid EDS mapping
  • Atomic resolution imaging of dynamic events using Gatan K2 IS (in situ) up to 1600fps
  • Fast STEM EELS and energy-filtered TEM mapping using Gatan GIF Quantum equipped with both CCD and K2 summit
  • 4D STEM capability using K2 IS (up to 1600fps)
  • K2 Summit for super high resolution (8K x 8K in super-resolution mode) low-dose imaging
  • Biprism for electron holography
  • In situ biasing, gas-solid reaction, and heating with atomic resolution STEM and TEM
  • Electron Tomography to study nanostructure in three dimensions

Popular Applications

  • Atomic resolution STEM imaging of various materials using various STEM detectors (HAADF, MAADF, BF, ABF, and BEI)
  • Atom-by-atom chemical analysis using EDS or EELS
  • Virtual STEM imaging and differential phase contrast (DPC) using 4D STEM
  • Atomic resolution imaging in S/TEM during an in-situ experiment
  • Low-dose imaging of beam-sensitive sample using K2 Summit
  • Atomic resolution gentle S/TEM of 2D materials at 60 and 80kV

Instrument Specifications

TEM information limit: 0.076 nm (300 kV), 0.087 nm (200 kV), 0.1 nm (80 kV) and 0.108 nm (60 kV)
STEM HAADF resolution: 0.063 nm (300 kV), 0.08 nm (200 kV), 0.1 nm (80 kV) and 0.136 nm (60 kV)
EELS Energy resolution: 0.34 eV (300 kV), 0.33 eV (200 kV), 0.31 eV (80 kV), 0.30 eV (60 kV).
EDS Energy resolution: 121.5 eV